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Balasubramanian, K.
- Characterization of Triglycine Sulfate (TGS) Crystals Grown in Water-soluble CdS Nanoparticles Dispersed in Water
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Authors
Affiliations
1 Department of Physics, The MDT Hindu College, Tirunelveli-627010, Tamilnadu, IN
2 Department of Physics, Aditanar College of Arts and Science, Tiruchendur-628216, Tamilnadu, IN
3 PRIST University, Thanjavur, Tamilnadu, IN
1 Department of Physics, The MDT Hindu College, Tirunelveli-627010, Tamilnadu, IN
2 Department of Physics, Aditanar College of Arts and Science, Tiruchendur-628216, Tamilnadu, IN
3 PRIST University, Thanjavur, Tamilnadu, IN
Source
Indian Journal of Science and Technology, Vol 3, No 1 (2010), Pagination: 41-43Abstract
Single crystals of Triglycine Sulfate (TGS) were grown in water and also were grown in water-soluble CdS nanoparticles dispersed in water by solution method with slow evaporation technique at room temperature. Watersoluble CdS nanoparticles were synthesized by microwave-assisted solution method using the precursors such as cadmium sulfate, thioglycolic acid and ethylene diamine and they were used for the growth of CdS-added TGS crystals. The grown crystals were characterized by XRD technique, UV-visible spectral studies, measurement of density, microhardness studies, atomic absorptions studies. The effect of Cd2+ ions on various properties of TGS crystals have been analyszed and reported.Keywords
Crystal Growth, XRD, TGS Crystals, CdS NanoparticlesReferences
- Ashok K. Batra, Mohan D. Aggarwal and Ravindra B. Lal (2003) Growth and characterization of doped DTGS crystals for infrared sensing devices. Materials Lett. 57, 3943-3948.
- Balamurugan N, Lenin M, Bhagavannarayana G, Ramasamy P (2007) Growth of TGS crystals using uniaxially solution-crystallization method of Sankaranarayanan-Ramasamy. Crystal Res. Technol. 42,151-156.
- Barglik-Chory Ch., Buchold D, Schmitt M, Kiefer W, Heske C, Kumpf C, Fuchs O, Weinhardt L, Stahl A, Umbach E, Lentze M, Geurts J and Muller G (2003) Synthesis, structure and spectroscopic characterization of water-soluble CdS nanoparticles. Chemical Physics Lett. 379, 443–451.
- Berbacaru C, Alexandru HV, Pintilie L, Dutu A, Logofatu B and Radulescu RC (2005) Doped versus pure TGS crystals. Materials Sci. Engg. B11, 141-146.
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- Raghavan CM, Sankar R, Mohan Kumar R, Jayavel R (2008) Effect of amino acid doping on the growth and ferroelectric properties of triglycine sulphate single crystals. Materials Res. Bull. 43, 305–311.
- Selvarajan P, Siva dhas ATH, Freeda TH and Mahadevan CK (2008) Growth, XRD and dielectric properties of triglycine sulpho-phosphate (TGSP) crystals added with magnesiumsulfate. Physica B. 403, 4205–4208.
- Selvarajan P, Das BN, Gon HB and Rao KV (1992) Dielectric properties of quenched and X- ray irradiated triglycine sulphate single crystals later excited with laser light. J. Mat. Sci. Lett. 11, 1312-1314.
- Sun X, Wang M, Pan QW, Shi W and Fang CS (1999) Study on the growth and properties of quanidine doped triglycine sulfate crystal. Cryst. Res. Technol. 34, 1251-1254.
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- New Algorithm to Address Confounding Problems in Taguchi Parameter Design – A Practical Study
Abstract Views :168 |
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Authors
Affiliations
1 Dr. M.G.R. Educational and Research Institute University, Chennai - 600095, Tamil Nadu, IN
2 Kalasalingam Academy of Research and Education, Krishnankoil - 626126, Tamil Nadu, IN
1 Dr. M.G.R. Educational and Research Institute University, Chennai - 600095, Tamil Nadu, IN
2 Kalasalingam Academy of Research and Education, Krishnankoil - 626126, Tamil Nadu, IN
Source
Indian Journal of Science and Technology, Vol 8, No 35 (2015), Pagination:Abstract
It is essential to operate all manufacturing processes at optimum levels to stay competitive in the global environment. Optimum prediction in manufacturing process involves lot of experimentation as it involves time and cost. Taguchi Parameter Design (PDE) is a design where optimum prediction is achieved in lesser experimental runs subject to the condition that there is no confounding effect. Confounding effect is a drawback of Taguchi PDE due to which many Taguchi experiments fail in confirmation tests at desired confidence level. RABAL Algorithm is 12 step structured approach, which uses Orthogonality concept and linear graph for Factors and Interaction allocation and uses certain rules based on statistical concepts by which the accurate result of Taguhi parameter design experiment is ensured. Sleeve synchronizer 1&2 hard turning is a bottleneck operation in a gear manufacturing line taken for research optimized for better cycle time using Taguchi PDE and RABAL algorithm. Feed rate in first and second cut is observed as significant factors at 95% confidence level and Optimal parametric setting is identified. Accuracy of results is confirmed through confirmation tests. RABAL Algorithm can be used along with Taguchi PDE to minimize the confounding effects there by accuracy of experimental results are improved and results are achieved right first time.Keywords
Confounding Effect, Hard Turning, RABAL Algorithm, Sleeve Synchronizer 1&2, Taguchi Parameter Design- Analysis of Crown Shrinkage in Gravity Die Cast Aluminium Alloy LM 13 Piston
Abstract Views :180 |
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Authors
Affiliations
1 Department of Mechanical Engineering, Dr. M. G. R. Educational and Research Institute University, Chennai - 600095, Tamil Nadu, IN
2 Department of Mechanical Engineering, Kalasalingam Academy of Research and Education, Krishnankoil - 626126, Tamil Nadu, IN
1 Department of Mechanical Engineering, Dr. M. G. R. Educational and Research Institute University, Chennai - 600095, Tamil Nadu, IN
2 Department of Mechanical Engineering, Kalasalingam Academy of Research and Education, Krishnankoil - 626126, Tamil Nadu, IN
Source
Indian Journal of Science and Technology, Vol 8, No 35 (2015), Pagination:Abstract
Background/Objectives: Optimization of process parameters to obtain shrinkage free engine piston based on Al-Si casting alloy LM 13 fabricated by gravity die casting. Method/Statistical Analysis: Experimental analysis of design and process parameters like riser sleeve size, center core temperature, pouring metal temperature and solidification time was carried out on Al-Si casting alloy LM 13 based engine piston fabricated by die casting technique. The die casting experiments with different solidification time 90, 120 and 150 seconds and volume of molten metal consumed by different sleeve size were carried out to obtain optimum conditions to produce shrinkage free engine pistons. The die casted engine piston were sectioned and checked for shrinkage at different design and process parameters. Results/Findings: The results showed that there is an effect of centre core temperature towards the shifting of shrinkage from the crown to riser. The center core temperature should not be maintained below 200°C and should be in the range of 200 - 238°C. But it cannot be concluded that the crown shrinkage is only due to the centre core temperature. The molten metal Al-Si is less dense as a liquid than as a solid so castings shrink upon cooling, which can leave a void at the last point to solidify. Risers prevent this by providing molten Al-Si alloy to the casting as it solidifies, so that the shrinkage forms in the riser and not the in engine piston casting. It was found that the size of sleeve size is indirectly proportional to the occurrence of crown shrinkage and increase in size of sleeve size reduces the chances of shrinkage. Engine piston section results showed the shrinkage shifting from casting to riser side by increasing the sleeve size. However the effect of different solidification time and pouring metal temperature was not so significant on the occurrence of shrinkage. Applications/Improvements: The optimized center core pin temperature and riser sleeve size successfully prevented the shrinkage formation in the Al-Si casting alloy LM 13 engine piston casting. This not only helps in improving the casting quality but also in increasing the production.Keywords
Al-Si Alloy, Engine Pistons, Gravity Die Casting, Shrinkage, Solidification Time- Application of Heuristics for Parallel Flow Line Scheduling Problem
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Authors
Affiliations
1 Dr. M. G. R. Educational and Research Institute, University, Chennai - 600107, Tamil Nadu, IN
2 Department of Mechanical Engineering, Kalasalingam Academy of Research and Education, Krishnankoil - 626126, Tamil Nadu, IN
1 Dr. M. G. R. Educational and Research Institute, University, Chennai - 600107, Tamil Nadu, IN
2 Department of Mechanical Engineering, Kalasalingam Academy of Research and Education, Krishnankoil - 626126, Tamil Nadu, IN